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HomeMy WebLinkAboutWater sample results test 2.pdfOctober 29, 2020 PBS Engineering & Environmental Pat Togher Attention Pat Togher: RE:Renton Mazda Work Order Number:2010443 214 E Galer St. Suite 300 Seattle, WA 98102 3600 Fremont Ave. N. Seattle, WA 98103 T: (206) 352-3790 F: (206) 352-7178 info@fremontanalytical.com Fremont Analytical, Inc. received 2 sample(s) on 10/27/2020 for the analyses presented in the following report. Brianna Barnes This report consists of the following: - Case Narrative - Analytical Results - Applicable Quality Control Summary Reports - Chain of Custody All analyses were performed consistent with the Quality Assurance program of Fremont Analytical, Inc. Please contact the laboratory if you should have any questions about the results. Thank you for using Fremont Analytical. Sincerely, Project Manager Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. Gasoline by NWTPH-Gx pH by SM 4500H+B Total Metals by EPA Method 200.8 Turbidity by EPA Method 180.1 Volatile Organic Compounds by EPA Method 8260D www.fremontanalytical.com Original DoD-ELAP Accreditation #79636 by PJLA, ISO/IEC 17025:2017 and QSM 5.3 for Environmental Testing ORELAP Certification: WA 100009 (NELAP Recognized) for Environmental Testing Washington State Department of Ecology Accredited for Environmental Testing, Lab ID C910 Page 1 of 17 10/29/2020Date: Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 Work Order Sample Summary Lab Sample ID Client Sample ID Date/Time ReceivedDate/Time Collected 2010443-001 Vault 10/27/2020 12:10 PM 10/27/2020 12:59 PM 2010443-002 Trip Blank 10/23/2020 2:35 PM 10/27/2020 12:59 PM Note: If no "Time Collected" is supplied, a default of 12:00AM is assigned Original Page 2 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental 10/29/2020 Case Narrative 2010443 Date: WO#: I. SAMPLE RECEIPT: Samples receipt information is recorded on the attached Sample Receipt Checklist. II. GENERAL REPORTING COMMENTS: Results are reported on a wet weight basis unless dry-weight correction is denoted in the units field on the analytical report ("mg/kg-dry" or "ug/kg-dry"). Matrix Spike (MS) and MS Duplicate (MSD) samples are tested from an analytical batch of "like" matrix to check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. The sample chosen for spike purposes may or may not have been a sample submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The LCS and the MB are processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire analytical process. III. ANALYSES AND EXCEPTIONS: Exceptions associated with this report will be footnoted in the analytical results page(s) or the quality control summary page(s) and/or noted below. Original Page 3 of 17 10/29/2020 Qualifiers & Acronyms 2010443 Date Reported: WO#: Qualifiers: * - Flagged value is not within established control limits B - Analyte detected in the associated Method Blank D - Dilution was required E - Value above quantitation range H - Holding times for preparation or analysis exceeded I - Analyte with an internal standard that does not meet established acceptance criteria J - Analyte detected below Reporting Limit N - Tentatively Identified Compound (TIC) Q - Analyte with an initial or continuing calibration that does not meet established acceptance criteria (<20%RSD, <20% Drift or minimum RRF) S - Spike recovery outside accepted recovery limits ND - Not detected at the Reporting Limit R - High relative percent difference observed Acronyms: %Rec - Percent Recovery CCB - Continued Calibration Blank CCV - Continued Calibration Verification DF - Dilution Factor DUP - Sample Duplicate HEM - Hexane Extractable Material ICV - Initial Calibration Verification LCS/LCSD - Laboratory Control Sample / Laboratory Control Sample Duplicate MB or MBLANK - Method Blank MDL - Method Detection Limit MS/MSD - Matrix Spike / Matrix Spike Duplicate PDS - Post Digestion Spike Ref Val - Reference Value REP - Sample Replicate RL - Reporting Limit RPD - Relative Percent Difference SD - Serial Dilution SGT - Silica Gel Treatment SPK - Spike Surr - Surrogate Original www.fremontanalytical.com Page 4 of 17 Project:Renton Mazda Client Sample ID:Vault Collection Date:10/27/2020 12:10:00 PM Matrix:Stormwater Client:PBS Engineering & Environmental Lab ID:2010443-001 Analyses Result Qual Units Date AnalyzedDFRL Analytical Report 10/29/2020 2010443 Date Reported: Work Order: Diesel and Heavy Oil by NWTPH-Dx/Dx Ext.Analyst:IHBatch ID: 30181 Diesel (Fuel Oil)10/28/2020 5:12:57 PM50.0 µg/L 1ND Heavy Oil 10/28/2020 5:12:57 PM100µg/L 1194 Surr: 2-Fluorobiphenyl 10/28/2020 5:12:57 PM50 - 150 %Rec 183.4 Surr: o-Terphenyl 10/28/2020 5:12:57 PM50 - 150 %Rec 167.4 Gasoline by NWTPH-Gx Analyst:KTBatch ID: 30170 Gasoline 10/28/2020 3:38:42 AM50.0 µg/L 1ND Surr: Toluene-d8 10/28/2020 3:38:42 AM65 - 135 %Rec 1100 Surr: 4-Bromofluorobenzene 10/28/2020 3:38:42 AM65 - 135 %Rec 1102 Volatile Organic Compounds by EPA Method 8260D Analyst:KTBatch ID: 30170 Vinyl chloride 10/28/2020 3:38:42 AM0.200 µg/L 1ND cis-1,2-Dichloroethene 10/28/2020 3:38:42 AM1.00 µg/L 1ND Benzene 10/28/2020 3:38:42 AM1.00 µg/L 1ND Trichloroethene (TCE)10/28/2020 3:38:42 AM0.500 µg/L 1ND Toluene 10/28/2020 3:38:42 AM1.00 µg/L 1ND Tetrachloroethene (PCE)10/28/2020 3:38:42 AM1.00 µg/L 1ND Ethylbenzene 10/28/2020 3:38:42 AM1.00 µg/L 1ND m,p-Xylene 10/28/2020 3:38:42 AM1.00 µg/L 1ND o-Xylene 10/28/2020 3:38:42 AM1.00 µg/L 1ND Surr: Dibromofluoromethane 10/28/2020 3:38:42 AM84.8 - 113 %Rec 1109 Surr: Toluene-d8 10/28/2020 3:38:42 AM88.5 - 110 %Rec 1105 Surr: 1-Bromo-4-fluorobenzene 10/28/2020 3:38:42 AM89.9 - 108 %Rec 1102 Total Metals by EPA Method 200.8 Analyst:COBatch ID: 30195 Arsenic 10/28/2020 4:25:18 PM1.00 µg/L 11.25 Cadmium 10/28/2020 4:25:18 PM0.200 µg/L 1ND Chromium 10/28/2020 4:25:18 PM1.00 µg/L 12.51 Lead 10/28/2020 4:25:18 PM0.500 µg/L 1ND pH by SM 4500H+B Analyst:EHBatch ID: R62886 Hydrogen Ion (pH)10/27/2020 1:16:33 PMpH17.95 Original Page 5 of 17 Project:Renton Mazda Client Sample ID:Vault Collection Date:10/27/2020 12:10:00 PM Matrix:Stormwater Client:PBS Engineering & Environmental Lab ID:2010443-001 Analyses Result Qual Units Date AnalyzedDFRL Analytical Report 10/29/2020 2010443 Date Reported: Work Order: Turbidity by EPA Method 180.1 Analyst:EHBatch ID: R62887 Turbidity 10/27/2020 1:17:17 PM0.200 NTU 12.51 Original Page 6 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT pH by SM 4500H+B 10/29/2020Date: Sample ID:MB-R62886 Batch ID:R62886 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:pH RL Client ID:MBLKW RunNo:62886 SeqNo:1262256 MBLKSampType: Hydrogen Ion (pH)8.35 Sample ID:LCS-R62886 Batch ID:R62886 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:pH RL Client ID:LCSW RunNo:62886 SeqNo:1262257 LCSSampType: Hydrogen Ion (pH)7.000 101 95 10507.07 Sample ID:2010443-001DDUP Batch ID:R62886 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:pH RL Client ID:Vault RunNo:62886 SeqNo:1262259 DUPSampType: Hydrogen Ion (pH)107.950 0.6278.00 Original Page 7 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Turbidity by EPA Method 180.1 10/29/2020Date: Sample ID:MB-R62887 Batch ID:R62887 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:NTU RL Client ID:MBLKW RunNo:62887 SeqNo:1262235 MBLKSampType: Turbidity 0.200ND Sample ID:LCS-R62887 Batch ID:R62887 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:NTU RL Client ID:LCSW RunNo:62887 SeqNo:1262236 LCSSampType: Turbidity 10.00 106 90 1100.200 010.6 Sample ID:2010443-001DDUP Batch ID:R62887 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:NTU RL Client ID:Vault RunNo:62887 SeqNo:1262238 DUPSampType: Turbidity 200.200 2.510 2.832.44 Original Page 8 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Total Metals by EPA Method 200.8 10/29/2020Date: Sample ID:2010432-001ADUP Batch ID:30195 Analysis Date:10/28/2020 Prep Date:10/28/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62950 SeqNo:1263547 DUPSampType: Cadmium 300.200 4.466 3.684.63 Chromium 301.00 165.4 2.86170 Sample ID:2010432-001AMS Batch ID:30195 Analysis Date:10/28/2020 Prep Date:10/28/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62950 SeqNo:1263548 MSSampType: Cadmium 25.00 99.8 70 1300.200 4.46629.4 Chromium 500.0 109 70 1301.00 165.4712 Sample ID:2010432-001AMSD Batch ID:30195 Analysis Date:10/28/2020 Prep Date:10/28/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62950 SeqNo:1263549 MSDSampType: Cadmium 25.00 109 70 130 300.200 4.466 29.41 7.2431.6 Chromium 500.0 109 70 130 301.00 165.4 711.7 0.394709 Sample ID:MB-30195 Batch ID:30195 Analysis Date:10/28/2020 Prep Date:10/28/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:MBLKW RunNo:62950 SeqNo:1263564 MBLKSampType: Cadmium 0.200ND Chromium 1.00ND Original Page 9 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Total Metals by EPA Method 200.8 10/29/2020Date: Sample ID:LCS-30195 Batch ID:30195 Analysis Date:10/28/2020 Prep Date:10/28/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:LCSW RunNo:62950 SeqNo:1263565 LCSSampType: Cadmium 5.000 106 85 1150.200 05.29 Chromium 100.0 110 85 1151.00 0110 Original Page 10 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. 10/29/2020Date: Sample ID:MB-30181 Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:MBLKW RunNo:62925 SeqNo:1263048 MBLKSampType: Diesel (Fuel Oil)49.2ND Heavy Oil 98.4ND Surr: 2-Fluorobiphenyl 78.73 84.6 50 15066.6 Surr: o-Terphenyl 78.73 71.3 50 15056.2 Sample ID:LCS-30181 Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:LCSW RunNo:62925 SeqNo:1263049 LCSSampType: Diesel (Fuel Oil)997.8 52.6 52 10749.9 0525 Surr: 2-Fluorobiphenyl 79.83 80.5 50 15064.2 Surr: o-Terphenyl 79.83 61.1 50 15048.8 Sample ID:2010450-003BDUP Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62925 SeqNo:1263631 DUPSampType: Diesel (Fuel Oil)3049.6 0ND Heavy Oil 3099.3 0ND Surr: 2-Fluorobiphenyl 79.43 84.0 50 150 066.8 Surr: o-Terphenyl 79.43 65.0 50 150 051.6 Sample ID:2010401-001AMS Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62925 SeqNo:1263639 MSSampType: Diesel (Fuel Oil)982.5 36.8 23.6 13049.1 33.27395 Surr: 2-Fluorobiphenyl 78.60 85.3 50 15067.0 Surr: o-Terphenyl 78.60 39.0 50 150 S30.6 Original Page 11 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Diesel and Heavy Oil by NWTPH-Dx/Dx Ext. 10/29/2020Date: Sample ID:2010401-001AMS Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62925 SeqNo:1263639 MSSampType: NOTES: S - Outlying surrogate recovery(ies) observed. Sample ID:2010418-001BDUP Batch ID:30181 Analysis Date:10/28/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62925 SeqNo:1263644 DUPSampType: Diesel (Fuel Oil)3049.6 46.29 17.054.9 Heavy Oil 3099.1 0ND Surr: 2-Fluorobiphenyl 79.30 97.6 50 150 077.4 Surr: o-Terphenyl 79.30 76.6 50 150 060.7 Original Page 12 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Gasoline by NWTPH-Gx 10/29/2020Date: Sample ID:LCS-30170 Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:LCSW RunNo:62916 SeqNo:1262856 LCSSampType: Gasoline 500.0 102 65 13550.0 0510 Surr: Toluene-d8 25.00 101 65 13525.2 Surr: 4-Bromofluorobenzene 25.00 103 65 13525.7 Sample ID:MB-30170 Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:MBLKW RunNo:62916 SeqNo:1262857 MBLKSampType: Gasoline 50.0ND Surr: Toluene-d8 25.00 99.9 65 13525.0 Surr: 4-Bromofluorobenzene 25.00 101 65 13525.2 Sample ID:2010414-001DDUP Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62916 SeqNo:1262848 DUPSampType: Gasoline 3050.0 0ND Surr: Toluene-d8 25.00 100 65 135 025.1 Surr: 4-Bromofluorobenzene 25.00 101 65 135 025.3 Sample ID:2010415-003ADUP Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62916 SeqNo:1262850 DUPSampType: Gasoline 3050.0 0ND Surr: Toluene-d8 25.00 100 65 135 025.0 Surr: 4-Bromofluorobenzene 25.00 102 65 135 025.4 Original Page 13 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Volatile Organic Compounds by EPA Method 8260D 10/29/2020Date: Sample ID:LCS-30170 Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:LCSW RunNo:62914 SeqNo:1262817 LCSSampType: Vinyl chloride 20.00 109 62.3 1480.200 021.8 cis-1,2-Dichloroethene 20.00 102 83.7 1221.00 020.5 Benzene 20.00 104 80.5 1261.00 020.7 Trichloroethene (TCE)20.00 98.9 75.5 1320.500 019.8 Toluene 20.00 105 82.9 1241.00 021.0 Tetrachloroethene (PCE)20.00 108 90.5 1211.00 021.6 Ethylbenzene 20.00 111 85.3 1231.00 022.3 m,p-Xylene 40.00 108 85.8 1221.00 043.2 o-Xylene 20.00 111 85.4 1211.00 022.3 Surr: Dibromofluoromethane 25.00 99.7 84.8 11324.9 Surr: Toluene-d8 25.00 98.3 88.5 11024.6 Surr: 1-Bromo-4-fluorobenzene 25.00 102 89.9 10825.6 Sample ID:MB-30170 Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:MBLKW RunNo:62914 SeqNo:1262818 MBLKSampType: Vinyl chloride 0.200ND cis-1,2-Dichloroethene 1.00ND Benzene 1.00ND Trichloroethene (TCE)0.500ND Toluene 1.00ND Tetrachloroethene (PCE)1.00ND Ethylbenzene 1.00ND m,p-Xylene 1.00ND o-Xylene 1.00ND Surr: Dibromofluoromethane 25.00 107 84.8 11326.7 Surr: Toluene-d8 25.00 104 88.5 11026.0 Surr: 1-Bromo-4-fluorobenzene 25.00 101 89.9 10825.2 Original Page 14 of 17 Project:Renton Mazda CLIENT:PBS Engineering & Environmental Work Order:2010443 QC SUMMARY REPORT Volatile Organic Compounds by EPA Method 8260D 10/29/2020Date: Sample ID:2010414-001DDUP Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62914 SeqNo:1262801 DUPSampType: Vinyl chloride 300.200 0ND cis-1,2-Dichloroethene 301.00 0ND Benzene 301.00 0ND Trichloroethene (TCE)300.500 0ND Toluene 301.00 0ND Tetrachloroethene (PCE)301.00 0ND Ethylbenzene 301.00 0ND m,p-Xylene 301.00 0ND o-Xylene 301.00 0ND Surr: Dibromofluoromethane 25.00 107 84.8 113 026.7 Surr: Toluene-d8 25.00 104 88.5 110 025.9 Surr: 1-Bromo-4-fluorobenzene 25.00 101 89.9 108 025.4 Sample ID:2010415-003ADUP Batch ID:30170 Analysis Date:10/27/2020 Prep Date:10/27/2020 Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimitHighLimit RPDLimit Qual Units:µg/L RL Client ID:BATCH RunNo:62914 SeqNo:1262805 DUPSampType: Vinyl chloride 300.200 0ND cis-1,2-Dichloroethene 301.00 0ND Benzene 301.00 0ND Trichloroethene (TCE)300.500 0ND Toluene 301.00 0ND Tetrachloroethene (PCE)301.00 0ND Ethylbenzene 301.00 0ND m,p-Xylene 301.00 0ND o-Xylene 301.00 0ND Surr: Dibromofluoromethane 25.00 108 84.8 113 027.0 Surr: Toluene-d8 25.00 105 88.5 110 026.2 Surr: 1-Bromo-4-fluorobenzene 25.00 102 89.9 108 025.5 Original Page 15 of 17 Date Received:10/27/2020 12:59:00 PM Client Name:PBS Work Order Number:2010443 Sample Log-In Check List Clare GriggsLogged by: Item Information How was the sample delivered?Client Is Chain of Custody complete?Yes No Not Present Was an attempt made to cool the samples?Yes No NA Are samples properly preserved?Yes No Was preservative added to bottles?Yes No NA Did all samples containers arrive in good condition(unbroken)?Yes No Does paperwork match bottle labels?Yes No Are matrices correctly identified on Chain of Custody?Yes No Is it clear what analyses were requested?Yes No Is there headspace in the VOA vials?Yes No NA 1. 2. 6. 10. 11. 12. 13. 14. 15. 16. 17.Were all holding times able to be met?Yes No Chain of Custody Log In 7.Were all items received at a temperature of >2°C to 6°C Yes No NA 8.Sample(s) in proper container(s)?Yes No 9.Sufficient sample volume for indicated test(s)?Yes No Special Handling (if applicable) 18. 19. Was client notified of all discrepancies with this order?Yes No NA Person Notified:Pat Togher Date:10/27/2020 Regarding:TAT pushed to 2 days Via:eMail Phone Fax In Person Additional remarks: Client Instructions:Acknowledged, proceed as soon as possible By Whom:Matt Langston Coolers are present?Yes No NA3. Unknown prior to receipt. Shipping container/cooler in good condition?Yes No4. Custody Seals present on shipping container/cooler? (Refer to comments for Custody Seals not intact) Yes No Not Present5. * Item #Temp ºC Sample 17.7 Page 1 of 1Note: DoD/ELAP and TNI require items to be received at 4°C +/- 2°C* Original Page 16 of 17 Page 17 of 17